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22423-26-3

  • Product Name：2,2'-Anhydro-5-methyluridine
  • Molecular Formula：C10H12N2O5
  • Purity：99%
  • Molecular Weight：240.216
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Product Details;

CasNo： 22423-26-3

Molecular Formula： C10H12N2O5

Appearance： Colourless solid

Reliable Quality Factory Sells For Sale 2,2'-Anhydro-5-methyluridine 22423-26-3

  • Molecular Formula:C10H12N2O5
  • Molecular Weight:240.216
  • Appearance/Colour:Colourless solid 
  • Melting Point:217.0 to 221.0 °C 
  • Boiling Point:452.0±55.0 °C at 760 mmHg 
  • PKA:12.56±0.60(Predicted) 
  • Flash Point:227.2±31.5 °C 
  • PSA：93.81000 
  • Density:1.9±0.1 g/cm3 
  • LogP:-1.43670 

22423-26-3 Relevant articles

Facile Synthesis of 5-Substituted Arabinofuranosyluracil Derivatives

Sawai, Hiroaki,Hayashi, Hidekazu,Sekiguchi, Sumie

, p. 605 - 606 (1994)

Arabinoaminooxazoline reacted readily wi...

Method for preparing β-thymidine

-

Paragraph 0096-0098; 0110, (2018/02/04)

The invention relates to a preparation m...

METHODS FOR THE PREVENTION AND TREATMENT OF MAJOR ADVERSE CARDIOVASCULAR EVENTS USING COMPOUNDS THAT MODULATE APOLIPOPROTEIN B

-

Paragraph 00639, (2016/03/22)

Provided herein, for example, are method...

A new straightforward synthesis of 2′,3′-didehydro-2′,3′-dideoxy-2′-(2″-(trimethylsilyl)ethylthio)thymidine, key intermediate for the synthesis of 2′-substituted thionucleosides

Oliveira, Maralise P.,Franco, Lucas L.,Lima, Maria C.A.,Sim?es, Cláudia M.O.,Galdino, Suely L.,Pitta, Ivan R.,Décout, Jean-Luc,Alves, Ricardo J.

, p. 816 - 821 (2015/04/14)

We describe herein a straightforward and...

Cu(I)-catalyzed efficient synthesis of 2'-triazolo-nucleoside conjugates

Mathur,Rana,Olsen,Parmar,Prasad

, p. 701 - 710 (2015/05/13)

A small library of thirty-two 2'-triazol...

22423-26-3 Process route

5-Methyluridine
1463-10-1,642082-80-2

5-Methyluridine

O-2,2'-cyclo-5-methyluridine
22423-26-3

O-2,2'-cyclo-5-methyluridine

Conditions
Conditions Yield
With sodium hydroxide; Diethyl carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 8h; Reagent/catalyst;
95.6%
With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 100 ℃;
90%
With bis(phenyl) carbonate; sodium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); for 1h; Heating / reflux;
85%
With sodium hydrogencarbonate; carbonic acid dimethyl ester; In N,N-dimethyl-formamide; at 130 ℃; for 2h;
78%
With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 150 ℃; for 0.5h;
64%
With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 130 ℃; for 0.5h;
62%
With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 150 ℃;
47%
With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide;
With bis(phenyl) carbonate; sodium hydrogencarbonate; Multistep reaction; 1.) HMPA, 70 deg C, 0.5 h, 2.) HMPA, 150 deg C, 2 h;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 150 ℃;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 1.5h; Heating;
With Ph2CO3;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); for 1h; Heating / reflux;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); for 1h; Heating / reflux;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 1h; Heating / reflux;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); for 1h; Heating / reflux;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); for 1h; Heating / reflux;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); for 1h; Heating / reflux;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); for 1h; Heating / reflux;
With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 1h; Reflux;
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

5-Methyluridine
1463-10-1,642082-80-2

5-Methyluridine

O-2,2'-cyclo-5-methyluridine
22423-26-3

O-2,2'-cyclo-5-methyluridine

Conditions
Conditions Yield
With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 1h; Heating / reflux;
85%
With sodium hydrogencarbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide;
With sodium hydrogencarbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide;
With sodium hydrogencarbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide;
With sodium hydrogencarbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide;
With sodium hydrogencarbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide;
With sodium hydrogencarbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide;
With sodium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); for 1h; Heating / reflux;

22423-26-3 Upstream products

  • 1463-10-1
    1463-10-1

    5-Methyluridine

  • 68-12-2
    68-12-2

    N,N-dimethyl-formamide

  • 52486-19-8
    52486-19-8

    1-(β-D-xylofuranosyl)-thymine

  • 512781-08-7
    512781-08-7

    1-(3,5-O-sulfinyl-β-D-xylofuranosyl)thymine

22423-26-3 Downstream products

  • 52259-53-7
    52259-53-7

    (3aS)-3c-hydroxy-2t-hydroxymethyl-7-methyl-(3ar,9ac)-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-8-one

  • 154534-68-6
    154534-68-6

    2'-deoxy-2'-methylthio-5-methyluridine

  • 95585-76-5
    95585-76-5

    2'-bromothymidine

  • 605-23-2
    605-23-2

    thymine arabinoside

CAS Index: 1 2 3 4 5 6 7 8 9

Chemical Name Index: A B C D E F G H I J K L M N O P Q R S T U V W X Y Z

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